Department of Chemistry & Biochemistry

AVANCE III 600 (2009)

Bruker AVANCE III 600 NMR spectrometer is a 14.1 Tesla narrow bored (54 mm) magnet with 2nd generation digital receiver, 100 W proton amplifier, 500 W broadband amplifier, a 10 Amp gradient amplifier, a VT unit, and a BCU-05 cooling unit with liquid N2 dewar and heat exchanger for operation down to -100 °C. All data are uploaded to the ChemSpec server for you to process on your personal computer.

Two probes are available:

  • Inverse triple resonance (TXI) probe (5 mm sample diameter) for observation of 1H while decoupling 13C and 15N. Autolock and autoshim capabilities. Variable temperature capabilities ranging from -50 °C to +80 °C.
  • Multinuclear broadband Fluorine Observe (BBFO) probe (5 mm sample diameter) with digital tuning covering the range from 15N to 31P and 19F with 1H decoupling. Variable temperature capabilities ranging from -80 °C to +130 °C.

The instrument is located in 121D Dobo Hall.  Enquiries should be directed to Dr. Shu-Yu (Aaron) Liao.

Acknowledgement of NSF Support - Instrument Purchase
"The AVANCE III 600 NMR spectrometer used to obtain results in this publication was supported by the National Science Foundation under Grant No. 0821552."

Acknowledgement of CheIF Staff Assistance
"The authors would like to acknowledge UNCW NMR/MS Facilities staffs <insert name(s) here> for the assitance of VANCE III 600 NMR spectrometer.”